Formulation challenges / Microencapsulation

Modified Starch Solutions for Microencapsulation

Plan your path from core material to powder. Explore starch wall-material selection for flavors, oils and oil-soluble ingredients, matched to feed preparation, spray drying and the intended application.

Emulsion preparationEncapsulation evaluationPowder performance
Golden nutritional oil beside fine lipid powder and a stainless steel scoop
01 / Identify the challenge

Is Your Encapsulated Powder Meeting Its Target?

Identify which result needs to improve. Encapsulation efficiency, core retention, powder recovery and reconstitution answer different questions.

01 / SURFACE OIL

Oil Appears on the Powder Surface

Use defined surface-oil and total-oil methods. Compare the wall system, loading and drying conditions before setting an acceptance target.

02 / CORE RETENTION

Core Retention Falls During Drying

Measure the core before and after drying on a consistent calculation basis. Account for the particular oil, flavor or active ingredient.

03 / POWDER RECOVERY

Powder Recovery Is Inconsistent

Record recovered powder, feed solids and equipment losses, including wall deposits. Assess the process alongside the formulation.

04 / RECONSTITUTION

Reconstitution Misses the Target

Define the intended medium, mixing conditions and use temperature. Compare wetting, dispersion, lumps and the reconstituted product.

02 / Understand the process

From a Prepared Emulsion to an Encapsulated Powder

Connect the feed emulsion, drying process and finished powder in one evaluation plan.

  1. 01Wall material hydration
  2. 02Core addition
  3. 03Homogenization
  4. 04Spray drying
  5. 05Powder evaluation

Prepare the Feed Emulsion

Define hydration, core dispersion, droplet size and feed viscosity. Review emulsification alongside the downstream powder requirements.

Build the Encapsulating Matrix

Use a wall system and drying process suited to the core. A dried particle may contain multiple dispersed core regions within a matrix.

Conceptual particle with several core regions embedded in a wall matrix

Conceptual illustration; not a microscopy image.

Evaluate the Finished Powder

Measure encapsulation and recovery separately. Include moisture, dispersion and storage tests relevant to the core and intended use.

03 / Find your application

Find Your Microencapsulation Application

Begin with the specific core material. Set quality targets around its behavior during processing, storage and final use.

Amber liquid pouring from a glass beaker into a shallow glass dish
Flavor ingredients

Flavors & Aromatic Oils

Define the volatile core and compare retention through drying, then assess flavor performance in the intended application.

Explore flavor applications →
Stainless steel scoop holding fine powder above a glass jar beside a golden oil vial
Lipid ingredients

Nutritional Oils

Review core loading, surface oil and powder properties. Establish oil-specific oxidation and storage measurements where relevant.

Explore nutritional oil applications →
Red and yellow capsules beside white supplement powder on a dark surface
Vitamin ingredients

Oil-Soluble Vitamins

Identify the specific vitamin and its formulation. Evaluate content through processing and storage alongside the final use requirements.

Explore vitamin applications →
Yellow, orange and red pigment powders beside an oil sample and a stainless steel scoop
Color ingredients

Oil-Soluble Pigments

Compare pigment content, dispersion and finished-product color. Match the test plan to the particular pigment and intended matrix.

Explore pigment applications →
04 / Select by conditions

Choose Wall Materials Around Your Core and Process

Share your core, wall system and process requirements to help narrow candidate grades and trial conditions.

Define Your Formulation and Processing Conditions

Selection factorInformation to shareEvaluation focus
Core materialCore identity, composition and target loadingCore-specific processing and quality needs
Wall systemCurrent starch, maltodextrin and other blended materialsPreparation and compatibility
Wall-to-core ratioMass ratio and calculation basisLoading, encapsulation and powder recovery
Feed propertiesTotal solids, viscosity, droplets and emulsion conditionFeed preparation and handling
Drying processEquipment, inlet/outlet temperature, feed and atomization settingsProcess-dependent powder performance
Powder targetEncapsulation, core content, moisture and dispersion requirementsMeasurable acceptance criteria
Storage & usePackaging, storage conditions and final applicationRelevant quality changes over time
Product family to discuss

E1450 / Starch Sodium Octenyl Succinate

Explore OSA-modified starch as part of a wall-material system. Discuss the specific grade, preparation requirements and intended application with Tianjiang.

View E1450 product information →
Start with the complete system

Match the Grade to Your Wall System

Share the core, current blend, feed conditions and powder target. Use application trials to establish the appropriate grade and formulation.

Discuss your wall-material system →

The modification type alone does not specify an encapsulation efficiency, storage life or universal blend ratio. Confirm suitability for the specific grade, core and process.

05 / Experiments & evaluation

Tianjiang’s Guide to Microencapsulation Evaluation

Compare loading and wall systems, then evaluate the powder against your own process and application targets.

Model Formulation and Drying Conditions

MCT oil core; 40% total solids. Each functional wall material was blended 1:1 with maltodextrin (MD). Premixing: 15,000 rpm, 3 min; homogenization: 500 bar, three passes. Spray-drying inlet: 150°C; outlet: 95 ± 5°C. Wall-to-oil ratios are mass ratios.

Comparison A / Loading

Compare Wall-to-Oil Ratios

OSA starch/MD system.

OSA starch/MD: wall-to-oil ratio comparison
Wall:oilEncapsulation efficiency (%)Powder yield (%)
1:183.92 ± 0.1988.57 ± 0.46
2:198.38 ± 0.0184.83 ± 3.98
3:198.87 ± 0.1984.22 ± 1.52

Balance the targetsEncapsulation efficiencies at 2:1 and 3:1 were not significantly different.

Comparison B / Wall system

Compare Blended Wall Systems

Fixed wall-to-oil ratio of 2:1.

Blended wall systems at 2:1 wall-to-oil ratio
Wall blendEncapsulation efficiency (%)Powder yield (%)
Gum arabic/MD83.95 ± 1.3682.54 ± 3.52
Whey protein isolate/MD89.60 ± 0.2986.51 ± 2.41
OSA starch/MD98.38 ± 0.0184.83 ± 3.98

Evaluate more than one resultThe two panels examine different factors in the same experimental design.

Read Encapsulation Efficiency and Yield Separately

Encapsulation efficiency (%)

(Total oil − surface oil) ÷ total oil × 100.

Powder yield (%)

Recovered powder mass ÷ initial feed solids mass × 100.

These model comparisons are not Tianjiang product specifications. Encapsulation efficiency alone does not demonstrate oxidation resistance, flavor retention or shelf life.

Build a Test Plan for Your Product

Evaluation areaInformation to recordComparison control
Feed emulsionDroplet distribution, viscosity, separation and holding timeSame conditioning and test methods
EncapsulationTotal core, surface core and the calculation methodCore-appropriate analytical procedure
Powder recoveryCollected powder, feed solids and equipment lossesConsistent recovery and mass basis
Powder propertiesMoisture, water activity, flow and cakingSame storage and sample handling
ReconstitutionWetting, dispersion and reconstituted product stateSame medium, mixing and temperature
Storage performanceCore content, oxidation, color or flavor as appropriateIntended packaging and storage conditions
06 / Plan your next step

From Core Material to Application Trial

Share Your Core and Target

Describe the core, current wall materials, process conditions and powder requirements.

Discuss Wall Material Options

Contact Tianjiang to review candidate grades, available technical information and sample needs.

Evaluate Your Powder

Compare powder properties and final application performance in your actual process.

07 / Common questions

Microencapsulation with Modified Starch: FAQs

What Is the Role of Modified Starch in Microencapsulation?

Discuss the specific starch grade as part of the wall-material system. Evaluate the feed emulsion, encapsulation performance and powder properties in the intended process.

How Is Microencapsulation Different from Emulsification?

Emulsification prepares an oil-and-water dispersion. Microencapsulation adds a further objective: incorporating the core into a matrix and evaluating the resulting powder. A successful feed emulsion alone does not confirm powder quality.

Can OSA Starch Be Blended with Maltodextrin?

OSA starch and maltodextrin can be considered as a blended wall system. Establish the blend ratio, total solids and preparation method through grade-specific technical information and application trials.

How Should the Wall-to-Core Ratio Be Selected?

Compare a defined range using the actual core, wall system and drying process. Balance encapsulation, loading, feed properties and powder recovery rather than choosing solely by one result.

Does High Encapsulation Efficiency Mean Longer Shelf Life?

Encapsulation efficiency does not by itself establish shelf life. Select storage measurements relevant to the core, such as content, oxidation, color or flavor, and use the intended packaging and conditions.

What Information Is Needed for a Recommendation?

Start with the core, target loading, current wall materials, feed solids, homogenization, drying conditions and desired powder properties. Include the intended application, packaging and storage requirements.

08 / Discuss your formulation

Find the Right Starch for Your Encapsulation System

Tell us what you want to encapsulate and how the powder will be used. Contact Tianjiang to discuss grade options, technical information and sample availability.

Helpful Details for Your Enquiry

  • Core material and target loading
  • Current wall materials and blend ratio
  • Feed solids and homogenization conditions
  • Spray-drying conditions
  • Powder targets and storage requirements

Not sure of every parameter? Start with what you know.

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